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Single-crystal X-ray diffractometer

Model
SC-XRD
Manufacturer
RIGAKU
Specification
This apparatus determines the three-dimensional arrangement of molecules and atoms by collecting and analyzing diffraction patterns obtained by irradiating a single crystal with X-rays. It can measure microcrystals down to a size of several tens of micrometers, which is approximately the lower limit for identifying crystal shapes under an optical microscope. Diffraction data collection typically takes around half a day to one day per sample on average. 
Location
UjiCampusMainBldg M166-C
Installation Year
2024
Overview

Rigaku single-crystal X-ray diffractometer (manufactured in 2024), equipped with a MicroMax-007 HF high-intensity X-ray generator (1.2 kW, 50 kV, 24 mA, Mo radiation), VariMax confocal X-ray optics, a HyPix-6000HE or PILATUS 200K detector, an Oxford Cryosystems Cobra low-temperature device (capable of cooling down to 80 K), and CrysAlisPro software for data collection and analysis. This apparatus determines the three-dimensional arrangement of molecules and atoms by collecting and analyzing diffraction patterns obtained by irradiating a single crystal with X-rays. It can measure microcrystals down to a size of several tens of micrometers, which is approximately the lower limit for identifying crystal shapes under an optical microscope. Diffraction data collection typically takes around half a day to one day per sample on average. 

Responsible department

Uji Campus Chemical Research Institute, Building M, Room M-116C

Available Users

Kyoto University
Use -by-the-hour
Accepted only between 9 am and 5 pm off campus

Other Research Institutes
Use -by-the-hour
Accepted only between 9 am and 5 pm off campus

Companies, etc.
Public offering

Notes

Prior to use, users must register as an X-ray apparatus operator at their affiliated institution, contact the staff in charge, and submit an application for X-ray work regarding this equipment in advance. In addition, a dosimeter must be worn when operating the equipment.

Usage rules
Inquiries

Organometallic Catalytic Chemistry, International Research Center for Elements Science, Institute for Chemical Research
(Contact: Tanifuji)
Email: tanifuji*scl.kyoto-u.ac.jp
※Please change 「*」 to 「@」 and send.

USACO website
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